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@PHDTHESIS{Zhang:459453,
author = {Zhang, Yan},
othercontributors = {Blümich, Bernhard},
title = {{S}patially resolved 2{D} {L}aplace {NMR}},
address = {Aachen},
publisher = {Publikationsserver der RWTH Aachen University},
reportid = {RWTH-CONV-145361},
pages = {86 S. : Ill., graph. Darst.},
year = {2014},
note = {Druckausg.: Zhang, Yan: Spatially resolved 2D Laplace NMR;
Aachen, Techn. Hochsch., Diss., 2014},
abstract = {Within the past decade, 2D Laplace nuclear magnetic
resonance (NMR) has been proved to be a powerful method to
investigate porous materials. However, it gives information
only about integral characteristics of a given sample with
regard to pore-size and pore connectivity. It is therefore
desirable to combine MRI with 2D-Laplace NMR to generate
information about fluid transport within defined areas of a
sample. Spatially resolved D-T2 correlation maps were
measured for four different samples: glass beads with
different bead diameters saturated with water, glass beads
filled with oil and water separated by a membrane, a wet
mortar sample and glass beads filled with oil and water
without a membrane. The information contained in pixels of
similar contrast were exploited by spatially resolved D-T2
correlation NMR as a representative of 2D-Laplace NMR.
Summation of pixels with similar contrast and low spatial
resolution have been chosen to accelerate the measurement
time which is inherently long for 2D-Laplace resolved MRI.
This method reveals the heterogeneous information of these
samples and is expected to be appreciated by the oil
industry. Moreover, Gint2D - T2 maps were obtained to study
the relationship between pore space and internal gradients
in porous media. Three different kinds of samples were
measured, which are glass beads with different bead
diameters saturated with water, glass beads filled with oil
and water, and a wet mortar sample. Two different cases are
distinguished: 1) The heterogeneity of internal gradients
dominates the heterogeneity of diffusion coefficients, which
concerns the first sample. 2) The heterogeneity of diffusion
coefficients dominates the heterogeneity of internal
gradients, which occurs in the second sample. Only in the
first case, the internal gradients can be estimated when
assuming a constant diffusion coefficient across the sample.
This result delineates the limitations of this assumption.
Then the correlation maps of mortar were measured and
internal gradient distributions were acquired to explore the
utility of this method in reality. Finally, spatially
resolved Gint2D - T2 maps were studied at 7 T and 16 T to
probe sample heterogeneity.},
keywords = {Poröser Stoff (SWD) / Kernspintomographie (SWD) /
Magnetische Kernresonanz (SWD) / Entspannung (SWD) /
Diffusion (SWD)},
cin = {150000 / 154110},
ddc = {540},
cid = {$I:(DE-82)150000_20140620$ / $I:(DE-82)154110_20140620$},
typ = {PUB:(DE-HGF)11},
urn = {urn:nbn:de:hbz:82-opus-52220},
url = {https://publications.rwth-aachen.de/record/459453},
}