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@MISC{Ksiazkiewicz:762101,
      author       = {Ksiazkiewicz, Agnieszka and Bering, Luise and Jung, Falco
                      Constantin and Wolter, Nadja Anna and Viell, Jörn and
                      Mitsos, Alexander and Pich, Andrij},
      title        = {{D}ata {S}et to „{C}losing the 1-5 µm {S}ize {G}ap:
                      {T}emperature-programmed, {F}ed-batch {S}ynthesis of
                      µm-sized {M}icrogels”},
      reportid     = {RWTH-2019-05397},
      year         = {2019},
      abstract     = {Microgels below 1 µm and above 20 µm are readily
                      accessible; however, obtaining them in size 1-10 µm still
                      remains a challenge. We present a surfactant-free
                      precipitation polymerization approach, combining
                      temperature-ramp (T-ramp) and fed-batch, generating 1-5 µm
                      in diameter poly(N-Vinylcaprolactam) (pVCL) microgels.
                      Confocal microscopy and dynamic light scattering (DLS)
                      confirm that the size of temperature-responsive pVCL
                      microgels can be adjusted by the feeding ratio. The
                      experimentally determined microgel sizes match well the
                      model-based predictions. The developed synthesis method
                      achieves high monomer conversions and provides high microgel
                      yields as determined by Raman spectroscopy.},
      cin          = {416710},
      cid          = {$I:(DE-82)416710_20140620$},
      pnm          = {SFB 985 B04 - Synthese von Mikrogelen: Kinetik,
                      Partikelbildung und Reaktordesign (B04) (221473487) / DFG
                      project 191948804 - SFB 985: Funktionelle Mikrogele und
                      Mikrogelsysteme (191948804)},
      pid          = {G:(GEPRIS)221473487 / G:(GEPRIS)191948804},
      typ          = {PUB:(DE-HGF)32},
      doi          = {10.18154/RWTH-2019-05397},
      url          = {https://publications.rwth-aachen.de/record/762101},
}