Gast ::
| 001 | 762101 | ||
| 005 | 20240701081739.0 | ||
| 024 | 7 | _ | |2 datacite_doi |a 10.18154/RWTH-2019-05397 |
| 037 | _ | _ | |a RWTH-2019-05397 |
| 041 | _ | _ | |a English |
| 100 | 1 | _ | |0 P:(DE-82)729328 |a Ksiazkiewicz, Agnieszka |b 0 |
| 245 | _ | _ | |a Data Set to „Closing the 1-5 µm Size Gap: Temperature-programmed, Fed-batch Synthesis of µm-sized Microgels” |
| 260 | _ | _ | |c 2019 |
| 336 | 7 | _ | |2 BibTeX |a MISC |
| 336 | 7 | _ | |0 PUB:(DE-HGF)32 |2 PUB:(DE-HGF) |a Dataset |b dataset |m dataset |s 1563879830_67650 |
| 336 | 7 | _ | |0 26 |2 EndNote |a Chart or Table |
| 336 | 7 | _ | |2 DataCite |a Dataset |
| 336 | 7 | _ | |2 ORCID |a DATA_SET |
| 336 | 7 | _ | |2 DINI |a ResearchData |
| 520 | _ | _ | |a Microgels below 1 µm and above 20 µm are readily accessible; however, obtaining them in size 1-10 µm still remains a challenge. We present a surfactant-free precipitation polymerization approach, combining temperature-ramp (T-ramp) and fed-batch, generating 1-5 µm in diameter poly(N-Vinylcaprolactam) (pVCL) microgels. Confocal microscopy and dynamic light scattering (DLS) confirm that the size of temperature-responsive pVCL microgels can be adjusted by the feeding ratio. The experimentally determined microgel sizes match well the model-based predictions. The developed synthesis method achieves high monomer conversions and provides high microgel yields as determined by Raman spectroscopy. |
| 536 | _ | _ | |0 G:(GEPRIS)221473487 |a SFB 985 B04 - Synthese von Mikrogelen: Kinetik, Partikelbildung und Reaktordesign (B04) (221473487) |c 221473487 |x 0 |
| 536 | _ | _ | |0 G:(GEPRIS)191948804 |a DFG project 191948804 - SFB 985: Funktionelle Mikrogele und Mikrogelsysteme (191948804) |c 191948804 |x 1 |
| 591 | _ | _ | |a Germany |
| 591 | _ | _ | |a Netherlands |
| 653 | _ | 7 | |a Microgels |
| 700 | 1 | _ | |0 P:(DE-82)IDM03320 |a Bering, Luise |b 1 |u rwth |
| 700 | 1 | _ | |0 P:(DE-82)IDM03100 |a Jung, Falco Constantin |b 2 |u rwth |
| 700 | 1 | _ | |0 P:(DE-HGF)0 |a Wolter, Nadja Anna |b 3 |
| 700 | 1 | _ | |0 P:(DE-82)IDM00357 |a Viell, Jörn |b 4 |u rwth |
| 700 | 1 | _ | |0 P:(DE-82)IDM00369 |a Mitsos, Alexander |b 5 |u rwth |
| 700 | 1 | _ | |0 P:(DE-82)IDM00066 |a Pich, Andrij |b 6 |e Corresponding author |u rwth |
| 787 | 0 | _ | |0 RWTH-2019-07407 |a Ksiazkiewicz, Agnieszka Natalia et.al. |d Amsterdam : Elsevier, 2019 |i RelatedTo |t Closing the 1-5 µm Size Gap: Temperature-programmed, Fed-batch Synthesis of µm-sized Microgels |
| 856 | 4 | _ | |u https://publications.rwth-aachen.de/record/762101/files/model_modelica.zip |y OpenAccess |
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| 914 | 1 | _ | |y 2019 |
| 915 | _ | _ | |0 StatID:(DE-HGF)0510 |2 StatID |a OpenAccess |
| 915 | _ | _ | |0 LIC:(DE-HGF)CC0 |2 HGFVOC |a CC0: Public Domain Dedication |
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