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@PHDTHESIS{Blankart:975531,
      author       = {Blankart, Charline},
      othercontributors = {Krupp, Ulrich and Brandt, Robert},
      title        = {{A}nwendbarkeit unterschiedlicher {W}ärmebehandlungsrouten
                      beim {P}resshärten von {M}ittelmanganstahl},
      school       = {Rheinisch-Westfälische Technische Hochschule Aachen},
      type         = {Dissertation},
      address      = {Aachen},
      publisher    = {RWTH Aachen University},
      reportid     = {RWTH-2023-12074},
      pages        = {1 Online-Ressource : Illustrationen},
      year         = {2023},
      note         = {Veröffentlicht auf dem Publikationsserver der RWTH Aachen
                      University 2024; Dissertation, Rheinisch-Westfälische
                      Technische Hochschule Aachen, 2023},
      abstract     = {Press-hardening of manganese-boron steels is one of the
                      most efficient production processes for high strength
                      automotive components. However, the residual formability of
                      these sheet components is greatly limited by the formation
                      of a fully martensitic microstructure. To extend the
                      application of press-hardened components also to impact
                      energy-absorptive parts of the vehicle body, the use of
                      third-generation advanced high strength steels, especially
                      medium manganese steels, is gaining increasing attention.
                      The alloying concept of these steels allows the critical
                      cooling rate and the Ac3-temperature to be significantly
                      lowered compared to manganese-boron steels, while
                      introducing a certain amount of retained austenite improves
                      the ductility of the material. Therefore, the present
                      research analyzes the application potential of
                      press-hardening of a medium manganese steel
                      (Fe-0,3C-5Mn-1,5Si) in combination with an intercritical
                      annealing or quenching $\&$ partitioning treatment. These
                      heat treatments lead in general to ultrafine-grained
                      multiphase microstructures containing retained austenite and
                      different body-centered cubic phases, such as fresh
                      martensite, tempered martensite, and ferrite, with different
                      carbon content each. Since, depending on the phase
                      fractions, strongly different mechanical properties are
                      expected, the qualitative distinction but also the
                      quantitative determination of the body-centered cubic phases
                      are of extraordinary importance to be able to understand the
                      correlation between microstructure and mechanical
                      properties. In the present study, it is shown that using
                      phase maps combined with grain average band slope of
                      electron backscatter diffraction measurements is a suitable
                      method to distinguish quantitatively fresh and tempered
                      martensite as well as martensite and ferrite which was
                      validated by electron probe micro analysis. Thermodynamic
                      simulation and dilatometer experiments were performed and
                      analyzed to understand the phase transformation kinetics of
                      Fe-0,3C-5Mn-1,5Si. Based on dilatation results and electron
                      backscatter diffraction analysis, the Koistinen-Marburger
                      equation was adapted to fit the investigated medium
                      manganese steel. According to the findings, suitable heat
                      treatment process windows for intercritical annealing and
                      quenching $\&$ partitioning were determined and reproduced
                      in both the dilatometer and salt baths. Regarding the
                      quenching $\&$ partitioning conditions, quenching
                      temperature has turned out to be an important influencing
                      parameter determining the phase fractions. It was shown that
                      an exceptional property combination of high strength and
                      ductility could be achieved when the phase fraction of fresh
                      martensite was less than $20\%,$ which was reached with a
                      quenching temperature ≤150 °C. Higher amounts of fresh
                      martensite lead, due to the difference in the plasticity of
                      the different phases, to increased stresses at the
                      interfaces and brittle intergranular fracture.Unlike the
                      quenching $\&$ partitioning conditions, the intercritically
                      annealed samples show discontinuous yielding behavior with
                      Lüders-plateau and serrations. The Lüders-plateau could
                      only be attenuated in the condition where also fresh
                      martensite, due to insufficient thermal stability of the
                      austenite, existed. Consequently, more mobile dislocations
                      were present in the microstructure, which carry the plastic
                      deformation. Selected heat treatments which reached
                      promising mechanical properties were reproduced in a
                      laboratory-scale press-hardening system equipped with a
                      heated hat-shaped tool. Even though the optimum temperature
                      range of quenching temperature could not yet be precisely
                      set in the press hardening tests carried out, initial
                      experiments show that a multiphase microstructure with
                      retained austenite fractions of more than $10\%$ can be
                      achieved by combining press hardening with quenching $\&$
                      partitioning. To match the optimum time for component
                      removal and thus achieve better mechanical properties, the
                      integration of improved sensor technology, is indispensable.
                      The evaluation of sensor data in combination with approaches
                      of integrated computational materials engineering would also
                      allow to predict properties based on process control and to
                      identify production scrap or to avoid it by an adapted heat
                      treatment.},
      cin          = {522110 / 520000},
      ddc          = {620},
      cid          = {$I:(DE-82)522110_20180901$ / $I:(DE-82)520000_20140620$},
      pnm          = {WS-B1.II-neu - Press Hardening (X080067-WS-B1.II-neu) / EXC
                      2023: Internet of Production (IoP)},
      pid          = {G:(DE-82)X080067-WS-B1.II-neu / G:(GEPRIS)390621612},
      typ          = {PUB:(DE-HGF)11},
      doi          = {10.18154/RWTH-2023-12074},
      url          = {https://publications.rwth-aachen.de/record/975531},
}