Dataset to: &quot;In-line Monitoring of Microgel Synthesis: Flow versus Batch Reactor&quot;

Kaven, Luise Friederike; Wolff, Hanna Josefine; Viell, Jörn; Wille, Lukas; Mitsos, Alexander; Wessling, Matthias

doi:10.18154/RWTH-2021-09666

Dataset to: "In-line Monitoring of Microgel Synthesis: Flow versus Batch Reactor"

Kaven, Luise Friederike^RWTH* ; Wolff, Hanna Josefine^RWTH* ; Wille, Lukas ; Wessling, Matthias^RWTH* ; Mitsos, Alexander^RWTH* ; Viell, Jörn^RWTH*

2021

Online
DOI: 10.18154/RWTH-2021-09666
URL: https://publications.rwth-aachen.de/record/834113/files/Raman_spectra_and_Indirect_Hard_Models.zip

Einrichtungen

Projekte

SFB 985 G02+ - In-line Monitoring von Mikrogel Produktionsprozessen (G02+) (221489508) (221489508)
DFG project 191948804 - SFB 985: Funktionelle Mikrogele und Mikrogelsysteme (191948804) (191948804)

Inhaltliche Beschreibung (Schlagwörter)
Raman spectroscopy (frei) ; in-line monitoring (frei) ; flow-chemistry (frei) ; microgel synthesis (frei)

Kurzfassung
This data set contains in-line Raman spectroscopy measurements inside a customized measurement cell for monitoring in a tubular flow reactor. The setup aims at monitoring the microgel synthesis in a flow reactor while aiming at a high measurement precision. The measurements include a systematic accuracy analysis, where different aspects of the flowing analyte are considered: solvent flow, flowing monomer solution, and flowing microgel solution. In addition, measurements for different calibration strategies are included. Lastly, this data set contains measurements of the microgel synthesis at varying residence times inside the tubular flow reactor.

OpenAccess:
ZIP
(additional files)